PREPARASI DAN KARAKTERISASI FILM TiO2 UNTUK REAKTOR FOTOKATALITIK FILM TiO2-UV

Gusfiyesi Gusfiyesi

Abstract

Preparasi dan karakterisasi film TiO2 untuk reaktor fotokatalitik film TiO2-UV telah dilakukan dalam penelitian ini. Film TiO2 yang paling optimum didapat saat dipreparasi dari suspensi TiO2 dan amilum dalam aquabidest dengan perbandingan (4 : 1: 25) wt.% yang dicoating dengan teknik screen-printing. Karakterisasi untuk sifat-sifat psikokimia dilakukan dengan XRD, TGA/SDTA, pengukuran Brunauer–Emmett–Teller (BET) dan SEM. Permukaan filmTiO2 yang diperoleh cukup merata ditunjukkan dari hasil analisis SEM dengan catalyst loading 0,0225 g/cm2 dan ketebalan ± 0,3 µm pada permukaan support keramik. Kata kunci: fotokatalitik, immobilisasi, film TiO2

References

. Yasumori, H. Shinoda, Y. Kameshima, S. Hayashi, K. Okada, 2001. Photocatalytic and Photoelectrochemical Properties of TiO2-Based Multiple Layer Thin Film Prepared by Sol–Gel and Reactive-Sputtering Methods, J. Mater. Chem. 11: 1253.

Arif, Syukri , Admin Alif, Nancy Willian, 2008. Pembuatan lapisan tipis TiO2-Doped logam (M=Ni, Cu dan Zn) dengan metoda dip-coating dan aplikasi sifat katalitiknya pada penjernihan air rawa gambut, J. Ris.Kim.: 2, No. 1

Bekbolet, M., Altan Serif Suphandag, Ceyda Senem Uyguner, 2002. An investigation of the photocatalytic efficiencies of TiO2 powders on the decolourisation of humic acids, Journal of Photochemistry and Photobiology A: Chemistry. 148: 121–128.

Gusfiyesi, Admin alif, Hermansyah Azis, Syukri Arif., 2015, Photocatalytic Degradation of Humic Acid with TiO2 Film Coated by Dipcoating Technique, The 8th Asia Pacific Symposium on Ion Analysis Proceeding, Online-September 2015

Hoffman, M. R. , S. T. Martin, W. Choi, D.W. Bahneman, Enviromental Aplication of semiconductors Photocatalysts. Chemical Review, 95(1): 71 – 74, (1995).

Mi-Hwa Baek, Ji-Sook Hong, Ji-Won Yoon, and Jeong-Kwon Suh, 2013., Photocatalytic Degradation of Humic Acid by Fe-supported on Spherical Activated Carbon with Enhanced Activity Light, International Journal of Photoenergy.

Palmer, P.L., Eggins, B.R., Coleman, H.M., 2002. The Effect of Operational Parameters on The Photocatalytic Degradation of Humic Acid, Journal of Photochemistry and Photobiology A: Chemistry, 148: 137–143.

Selcuk, H. and Bekbolet, M., 2008. Photocatalytic and photoelectrocatalytic humic acid removal and selectivity of TiO2 coated photoanode, Chemosphere, 73, 5, 854.

Sun, X.; Zhang, G.; Pan, X. 2012. Preparation and characteristics of TiO2 nanotube catalysts used in hybrid photocatalysis/membrane process. Catal. Commun. 18 : 76-80.

Uyguner, C.S. and Bekbolet M. 2010. TiO2-assisted photodegradation of humic acids: effect of copper ions, Water Science and Technology. 61: 10, 2581.

Uyguner, C.S. and Bekbolet, M., 2005. A comparative study on the photocatalytic degradation of humic substances of various origins, Desalination, 176: 167.

Wang,J.,Zhou,Y.,Li,A.,Xu,L., 2010. Adsorption of humic acid by bi-functional resin JN-10 and the effect of alkali-earth metal ions on the adsorption. J.Hazard. Mater. 176,1018–1026.

X. Zhao et al., 2004. Different Effects of Humic Substances on Photodegradation of p,p_-DDT on Soil Surfaces in The Presence of TiO2 Under UV and Visible Light, Journal of Photochemistry and Photobiology A: Chemistry 167: 177–18

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